SYNTHESIS AND X-RAY STRUCTURAL CHARACTERIZATION OF THE 1-1 ADDUCT OF BISMUTH(III) WITH THE SALTREN ANION [SALTREN-EQUIVALENT-TO-N(CH2CH2N=CHC6H4OH)3] - A NOVEL 7-COORDINATE BISMUTH(III) COMPLEX

被引:9
作者
BHARADWAJ, PK [1 ]
LEE, AM [1 ]
MANDAL, S [1 ]
SKELTON, BW [1 ]
WHITE, AH [1 ]
机构
[1] UNIV WESTERN AUSTRALIA,DEPT CHEM,NEDLANDS,WA 6009,AUSTRALIA
关键词
D O I
10.1071/CH9941799
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The synthesis and single-crystal X-ray structure determination of the title compound are recorded; crystals are monoclinic, P2(1)/c, a 10.309(8), b 18.817(7), c 15.542(6) angstrom, beta 121.80(5)-degrees-, Z 4; R was 0.038 for 2894 independent, 'observed' [I > 3delta(I)] reflections. The molecule has quasi-3 symmetry, with seven-coordinate bismuth [Bi-N(apical), 2.82(1); Bi-N, 2.512(8)-2.563(9); Bi-O, 2.197(8)-2.300(8) angstrom].
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页码:1799 / 1803
页数:5
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