STRUCTURAL STUDIES IN THE BICYCLO [3.1.1]HEPTANE SERIES BY H-1 AND C-13 NMR

被引：33

作者：

BADJAHHADJAHMED, AY

MEKLATI, BY

WATON, H

PHAM, QT

机构：

[1] UNIV SCI & TECHNOL HOUARI BOUMEDIENNE,INST CHIM,ANAL ORGAN FONCT LAB,BP 32,16111 EL ALIA,ALGERIA

[2] CNRS,SERV CENT ANAL,F-69390 VERNAISON,FRANCE

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1992年 / 30卷 / 09期

关键词：

H-1 AND C-13 NMR; BICYCLO[3.1.1]HEPTANE DERIVATIVES; PINANE COMPOUNDS; CONFORMATIONAL ANALYSIS;

D O I：

10.1002/mrc.1260300902

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The H-1 and C-13 NMR spectra of 22 pinane derivatives have been recorded and completely assigned. The spectral data for this set of compounds provide information about the conformation of these molecules and allow the deduction of the various structural effects observed in the bicyclo[3.1.1]heptane series.

引用

收藏

页码：807 / 816

页数：10

相关论文

共 42 条

[1] SUBSTITUENT CHEMICAL-SHIFTS IN NMR .4. - H-1 SCS IN SOME 2-SUBSTITUTED NORBORNANES AND BORNANES [J].

ABRAHAM, RJ ;

BARLOW, AP ;

ROWAN, AE .

MAGNETIC RESONANCE IN CHEMISTRY, 1989, 27 (11) :1074-1084

[2] NUCLEAR MAGNETIC RESONANCE LINE-SHAPE AND DOUBLE-RESONANCE STUDIES OF RING INVERSION IN CYCLOHEXANE-D11 [J].

ANET, FAL ;

BOURN, AJR .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1967, 89 (04) :760-&

[3]

ANET FAL, 1971, CONFIGURATION CONFOR, P388

[4] C-13, H-1 spin-spin coupling. X-Norbornane: A reinvestigation of the karplus curve for (3)J(C-13, H-1) [J].

AYDIN, R ;

GUNTHER, H .

MAGNETIC RESONANCE IN CHEMISTRY, 1990, 28 (05) :448-457

[5] NUCLEAR SPIN-SPIN COUPLING VIA NONBONDED INTERACTIONS .6. THE IMPORTANCE OF BRIDGEHEAD INTERACTIONS ON H-1-H-1, H-1-C-13, AND C-13-C-13 COUPLING-CONSTANTS IN BICYCLOALKANES [J].

BARFIELD, M ;

DELLA, EW ;

PIGOU, PE .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1984, 106 (18) :5051-5054

[6]

BAUM MW, 1982, TETRAHEDRON LETT, P31

[7]

BESSIERE.Y, 1970, B SOC CHIM FR, P3103

[8] PROTON MAGNETIC RESONANCE STUDIES OF CYCLIC COMPOUNDS .4. INFLUENCE OF ALKYL SUBSTITUENTS ON CHEMICAL SHIFTS OF RING PROTONS IN CYCLOHEXANE COMPOUNDS [J].

BOOTH, H .

TETRAHEDRON, 1966, 22 (02) :615-&

[9] NMR STUDY OF ROTATIONAL BARRIERS + CONFORMATIONAL PREFERENCES .2. D11-CYCLOHEXANE [J].

BOVEY, FA ;

ANDERSON, EW ;

KORNEGAY, RL ;

HOOD, FP .

JOURNAL OF CHEMICAL PHYSICS, 1964, 41 (07) :2041-&

[10] STRUCTURAL STUDIES IN THE CEDRANE SERIES BY C-13 NMR [J].

BRUN, P ;

CASANOVA, J ;

RAJU, MS ;

WAEGELL, B ;

WENKERT, E ;

ZAHRA, JP .

MAGNETIC RESONANCE IN CHEMISTRY, 1987, 25 (07) :619-627

← 1 2 3 4 5 →