SYNTHESIS OF BENZO-13-CROWN-4 DERIVATIVES

被引：5

作者：

CZECH, BP

ZAZULAK, W

KUMAR, A

DALLEY, NK

JIANG, WM

BARTSCH, RA

机构：

[1] BRIGHAM YOUNG UNIV,DEPT CHEM,PROVO,UT 84602

[2] TEXAS TECH UNIV,DEPT CHEM & BIOCHEM,LUBBOCK,TX 79409

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1991年 / 28卷 / 05期

关键词：

D O I：

10.1002/jhet.5570280534

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A series of nine, new benzo-13-crown-4 compounds which bear one or two substituents on the three-carbon bridge has been prepared in good yields by cesium fluoride-assisted cyclization reactions of catechol with ditosylates of the appropriate glycols. The solid state structure of 9,9-dibenzyl-2,3-benzo-13-crown-4 is determined and compared with the reported structure for the unsubstituted crown ether.

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页码：1387 / 1394

页数：8

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