THE CONFIRMATION AND QUANTITATION OF LSD IN URINE USING GAS-CHROMATOGRAPHY MASS-SPECTROMETRY

被引:7
作者
BUKOWSKI, N [1 ]
EATON, AN [1 ]
机构
[1] FISONS INSTRUMENTS INC,VG MASSLAB,MANCHESTER M23 9BE,ENGLAND
关键词
D O I
10.1002/rcm.1290070122
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Confirmation and quantitation of LSD, as its trimethyl silyl derivative, is carried out using a commercial gas chromatography/mass spectrometry system. The method uses 4 times less sample than previous methods, extends column life by reducing the amount of derivatizing agent used and can detect and quantify LSD at the 10 pg mL-1 level.
引用
收藏
页码:106 / 108
页数:3
相关论文
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[1]   GAS-CHROMATOGRAPHIC ELECTRON-IMPACT MASS FRAGMENTOMETRIC DETERMINATION OF LYSERGIC-ACID DIETHYLAMIDE IN URINE [J].
PAUL, BD ;
MITCHELL, JM ;
BURBAGE, R ;
MOY, M ;
SROKA, R .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1990, 529 (01) :103-112