INSTRUMENTATION AND CELL DESIGN FOR INSITU STUDIES OF ELECTRODE SURFACES USING X-RAY SYNCHROTRON RADIATION

被引：29

作者：

HERRON, ME

DOYLE, SE

ROBERTS, KJ

ROBINSON, J

WALSH, FC

机构：

[1] UNIV STRATHCLYDE,DEPT PURE & APPL CHEM,GLASGOW G1 1XL,SCOTLAND

[2] UNIV WARWICK,DEPT PHYS,COVENTRY CV4 7AL,W MIDLANDS,ENGLAND

[3] PORTSMOUTH POLYTECH,DEPT CHEM,APPL ELECTROCHEM GRP,PORTSMOUTH PO1 2DT,ENGLAND

[4] SERC,DARESBURY LAB,WARRINGTON WA4 4AD,CHESHIRE,ENGLAND

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 1992年 / 63卷 / 01期

关键词：

D O I：

10.1063/1.1143789

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

As an integral part of a program to develop x-ray techniques for in situ structural studies of electrode surfaces, a series of experiments has been carried out using x-ray diffraction (XRD) and x-ray absorption spectroscopy (XAS) at the Daresbury SRS. These studies, which involve continuous control of the electrode potential and the need to probe the electrode surface with synchrotron radiation, demand careful attention to cell design. Three types of experiment are described in order to illustrate possible approaches to cell design and the versatility of in situ x-ray techniques.

引用

页码：950 / 955

页数：6

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