SINGLE-CRYSTAL STRUCTURE OF K3NB8O21

被引:5
作者
BENABBAS, A [1 ]
BOREL, MM [1 ]
GRANDIN, A [1 ]
LECLAIRE, A [1 ]
RAVEAU, B [1 ]
机构
[1] CRISMAT ISMRA,CRISTALLOG & SCI MAT LAB,CNRS,BLVD MARECHAL JUIN,F-14050 CAEN,FRANCE
关键词
D O I
10.1107/S0108270192008916
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Tripotassium 21-oxooctaniobate, M(r) = 1196.53, hexagonal, P6(3)/mcm, a = 9.1584(5), c = 12.0404 (4) angstrom, V = 874.6 (1) angstrom3, Z = 2, D(x) = 4.54 Mg m-3, lambda(Mo Kalpha) = 0.71073 angstrom, mu = 5.65 mm-1, F(000) = 1106, T = 294 K, R = 0.044, wR = 0.047 for 2540 reflections with I > 3sigma(I). The framework is built up from [Nb6O24] units stacke along c giving [Nb6O21]infinity chains which are held together by single NbO6 octahedra.
引用
收藏
页码:439 / 441
页数:3
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