This paper uses an acoustic technique to determine the concentration profile developing during the sedimentation of noncolloidal bidisperse suspensions of glass beads in a Newtonian fluid. Various bead diameter ratios have been used and a wide range of relative concentrations is covered. From the shock front velocities and the concentrations in different zones, the sedimentation velocities of small and large particles in a homogeneous suspension of respective concentrations cs0 and c10 have been determined. The semidilute regime (c0=ss0+c 10<20%) has many similarities with the dilute regime, where large particles provide the dominant hydrodynamic hindrance to settling. In the concentrated regime (c0>35%), a mutual hindrance leads to a velocity reduction of large particles and to an enhancement of small ones, as compared to a monodisperse suspension. The data clearly demonstrate that size segregation in the concentrated regime disappears at a critical concentration, which for the size ratio 1.68 is equal to c0=45%. © 1994 American Institute of Physics.