C-13-H-1 SHIFT CORRELATION WITH FULL H-1-H-1 DECOUPLING

被引：34

作者：

PERPICKDUMONT, M

REYNOLDS, WF

ENRIQUEZ, RG

机构：

[1] UNIV TORONTO,DEPT CHEM,TORONTO M5S 1A1,ONTARIO,CANADA

[2] NATL AUTONOMOUS UNIV MEXICO,INST QUIM,MEXICO CITY 04510,DF,MEXICO

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1988年 / 26卷 / 05期

关键词：

D O I：

10.1002/mrc.1260260503

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A pulse sequence for obtaining 13C-1H shift-correlated spectra with full 1H-1H decoupling is described and evaluated. It is concluded that the sequence provides excellent resolution, even for strongly coupled methylene groups. The sensitivity is superior to those of existing sequences based on 13C detection for organic compounds in the molecular weight range up to ca 500. © 1988 John Wiley & Sons, Ltd.

引用

页码：358 / 361

页数：4

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