SYNTHESIS OF (1,2-BENZENEDIOLATO(2-)-0,0')OXOBIS(1-PIPERIDINOLATO(1-)-0,N)MOLYBDENUM(VI), [MOO(C5H10NO)2(C6H4O2)], AND STRUCTURE DETERMINATION BY CORRELATED H-1-C-13 TWO-DIMENSIONAL NMR-SPECTROSCOPY AND X-RAY CRYSTALLOGRAPHY

被引:30
作者
BRISTOW, S
ENEMARK, JH
GARNER, CD
MINELLI, M
MORRIS, GA
ORTEGA, RB
机构
[1] UNIV ARIZONA,DEPT CHEM,TUCSON,AZ 85721
[2] UNIV MANCHESTER,DEPT CHEM,MANCHESTER M13 9PL,LANCS,ENGLAND
关键词
D O I
10.1021/ic00218a022
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
引用
收藏
页码:4070 / 4077
页数:8
相关论文
共 41 条
[1]   2-DIMENSIONAL SPECTROSCOPY - APPLICATION TO NUCLEAR MAGNETIC-RESONANCE [J].
AUE, WP ;
BARTHOLDI, E ;
ERNST, RR .
JOURNAL OF CHEMICAL PHYSICS, 1976, 64 (05) :2229-2246
[2]   AN IMPROVED METHOD FOR HETERONUCLEAR CHEMICAL-SHIFT CORRELATION BY TWO-DIMENSIONAL NMR [J].
BAX, A ;
MORRIS, GA .
JOURNAL OF MAGNETIC RESONANCE, 1981, 42 (03) :501-505
[3]   CORRELATION OF PROTON CHEMICAL-SHIFTS BY TWO-DIMENSIONAL FOURIER-TRANSFORM NMR [J].
BAX, A ;
FREEMAN, R ;
MORRIS, G .
JOURNAL OF MAGNETIC RESONANCE, 1981, 42 (01) :164-168
[4]  
BAX A, 1982, 2 DIMENSIONAL NMR SP
[5]   C-13 AND PROTON TWO-DIMENSIONAL NMR-STUDY OF THE ORMOSIA ALKALOIDS PANAMINE, ORMOSANINE, AND ORMOSININE [J].
BHACCA, NS ;
BALANDRIN, MF ;
KINGHORN, AD ;
FRENKIEL, TA ;
FREEMAN, R ;
MORRIS, GA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1983, 105 (09) :2538-2544
[6]   LIGATION BY A CIS-DITHIO-MOLYBDENUM(VI) MOIETY - PREPARATION AND CRYSTAL-STRUCTURE OF [((PIPERIDINE-N-OXIDE(1-))2MO-(MU-2-S)2CU-MU-2-CL)2] [J].
BRISTOW, S ;
GARNER, CD ;
CLEGG, W .
INORGANICA CHIMICA ACTA-LETTERS, 1983, 76 (5-6) :L261-L262
[7]   COMPARATIVE ELECTROCHEMISTRY OF CIS-MOOS2+, MOO22+, AND MOS22+ CENTERS IN COMPLEXES OF THE TYPE CIS-[MOY2L2] (Y = O AND OR S, HL = 1-HYDROXYPIPERIDINE) - COMMENTS ON ACTIVE AND DESULFO-FORMS OF XANTHINE-OXIDASE AND XANTHINE DEHYDROGENASE [J].
BRISTOW, S ;
GARNER, CD ;
PICKETT, CJ .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1984, (08) :1617-1619
[8]   CRYSTAL-STRUCTURE OF THE COMPLEX CIS-OXOBIS[PIPERIDINE N-OXIDO(1-)-NO]THIOMOLYBDENUM(VI), CONTAINING A CIS-MOOS2+ GROUP [J].
BRISTOW, S ;
COLLISON, D ;
GARNER, CD ;
CLEGG, W .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1983, (11) :2495-2499
[9]   CRYSTAL STRUCTURE OF CATECHOL [J].
BROWN, CJ .
ACTA CRYSTALLOGRAPHICA, 1966, 21 :170-&
[10]   BIS[O-METHYL (S)-PENICILLAMINATO]-CIS-DIOXOMOLYBDENUM(VI), [MOO2((S)-PEN-OME)2] - STRUCTURE AND SPECTROSCOPIC STUDIES [J].
BUCHANAN, I ;
GARNER, CD ;
CLEGG, W .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1984, (07) :1333-1342