A SIMPLE, RAPID AND SIMULTANEOUS ANALYSIS OF COMPLEX VOLATILE HYDROCARBON MIXTURES IN BLOOD USING GAS-CHROMATOGRAPHY MASS-SPECTROMETRY WITH A WIDE-BORE CAPILLARY COLUMN

被引：9

作者：

MORINAGA, M ^{[1
]}

HARA, K ^{[1
]}

KAGEURA, M ^{[1
]}

HIEDA, Y ^{[1
]}

TAKAMOTO, M ^{[1
]}

KASHIMURA, S ^{[1
]}

机构：

[1] FUKUOKA UNIV,SCH MED,DEPT LEGAL MED,7-45-1 NANAKUMA,JONAN KU,FUKUOKA 81401,JAPAN

来源：

ZEITSCHRIFT FUR RECHTSMEDIZIN-JOURNAL OF LEGAL MEDICINE | 1990年 / 103卷 / 08期

关键词：

screening method; Volatile hydrocarbons in the blood;

D O I：

10.1007/BF01261420

中图分类号：

DF [法律]; D9 [法律]; R [医药、卫生];

学科分类号：

0301 ; 10 ;

摘要：

A screening method for detecting volatile hydrocarbons in blood has been developed using gas chromatography/mass spectrometry with a wide-bore capillary column and a headspace method. Toluene-d8 and indan were used as the internal standards for quantitative analysis. Hydrocarbons with retention indices from 600 to 1200 were simultaneously and quantitatively detected in relatively low concentrations (0.01 μg/m1) in reconstructed ion chromatography. This method could prove useful in forensic cases in which urgent examination of complex hydrocarbon mixtures, e.g. petroleum components, is required. © 1990 Springer-Verlag.

引用

页码：567 / 572

页数：6

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