AN EFFICIENT INEXPENSIVE ELECTROCHEMICAL PREPARATION OF RUPPERTS REAGENT

被引：18

作者：

AYMARD, F

NEDELEC, JY

PERICHON, J

机构：

[1] Laboratoire d'Electrochimie, Catalyse et Synthèse Organique CNRS, 94320 Thiais, 2, Rue Henri Dunant

来源：

TETRAHEDRON LETTERS | 1994年 / 35卷 / 46期

关键词：

D O I：

10.1016/S0040-4039(00)78453-X

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The electrochemical reduction of CF3Br in N,N-dimethylformamide (DMF) in the presence of Me(3)SiCl and a sacrificial aluminum anode provides Me(3)SiCF(3) in ca 90% faradaic yields.

引用

页码：8623 / 8624

页数：2

共 16 条

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