DETERMINATION OF CONFIGURATIONS OF LACTIC AND GLYCERIC ACIDS FROM HUMAN-SERUM AND URINE BY CAPILLARY GAS-LIQUID-CHROMATOGRAPHY

被引：54

作者：

KAMERLING, JP

GERWIG, GJ

VLIEGENTHART, JFG

DURAN, M

KETTING, D

WADMAN, SK

机构：

[1] STATE UNIV UTRECHT, ORGAN CHEM LAB, UTRECHT, NETHERLANDS

[2] STATE UNIV UTRECHT, HET WILHELMINA ZINDERZIEKENHUIS, UTRECHT, NETHERLANDS

来源：

JOURNAL OF CHROMATOGRAPHY | 1977年 / 143卷 / 02期

关键词：

D O I：

10.1016/S0378-4347(00)81817-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The separation of the enantiomers of lactic and glyceric acids can be achieved by capillary gas chromatography on SP-1000 using the corresponding O-acetylated menthyl esters. The structures of the derivatives were proved by PMR spectroscopy and mass spectrometry. The method was used for the determination of the absolute configurations of lactic and glyceric acids isolated from serum and urine from different patients.

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页码：117 / 123

页数：7

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