SLURRY ATOMIZATION DIRECT FLAME EMISSION DETERMINATION OF NA AND K IN HOT DOGS

被引:12
作者
FIETKAU, R
WICHMAN, MD
FRY, RC
机构
关键词
SODIUM COMPOUNDS;
D O I
10.1366/0003702844554189
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A slurry atomization method is presented for rapid, cost-effective, near-direct determinations of sodium and potassium in hot dogs by flame emission. Samples were briefly homogenized in water. Na and K were thereby solubilized. Hot dog slurries were directly introduced with a Babington nebulizer into a clog-free air-natural-gas burner. This cool flame eliminated ionization. Instrumental calibration was performed merely with separate aqueous standard solutions of NaCl and KCl. Ionization suppressants, internal standards, standard additions, matrix correction factors, matrix modifiers and matrix matching schemes were all found to be unnecessary for hot dog slurries directly analyzed with this system. The overall slurry atomization method eliminated the need for acids, fume hoods and lengthy sample preparation such as wet or dry ashing.
引用
收藏
页码:118 / 124
页数:7
相关论文
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