FLAME AAS DETERMINATION OF AS, CD AND TL IN SOILS AND SEDIMENTS AFTER THEIR SIMULTANEOUS CARBODITHIOATE EXTRACTION

被引:12
作者
IVANOVA, E
STOIMENOVA, M
GENTCHEVA, G
机构
[1] Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences, Sofia
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1994年 / 348卷 / 04期
关键词
D O I
10.1007/BF00324041
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The extraction system ammonium tetramethylenecarbodithioate/isobutylmethylketone is applied to the simultaneous preconcentration of the toxic trace elements As, Cd and T1 from soil digests at an acidity of 2-3 mol/l sulphuric acid and to their separation from the major soil components. The extraction procedure is easily coupled to AAS. The accuracy of the method is checked by the analysis of a certified reference material. RSD is between 4 and 10%.
引用
收藏
页码:317 / 319
页数:3
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