MEASUREMENT OF LIKE-SPIN DIPOLE COUPLINGS

被引:40
作者
LIZAK, MJ [1 ]
GULLION, T [1 ]
CONRADI, MS [1 ]
机构
[1] WASHINGTON UNIV,DEPT CHEM,ST LOUIS,MO 63130
来源
JOURNAL OF MAGNETIC RESONANCE | 1991年 / 91卷 / 02期
基金
美国国家科学基金会;
关键词
D O I
10.1016/0022-2364(91)90190-5
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The application of modified Carr-Purcell-type pulse sequences to the measurement of like-spin dipole couplings in solids is reported here. The Meiboom-Gill sequence is shown experimentally to be very sensitive to nutation angle errors. Previously reported modifications of the sequence are significantly more tolerant of pulse errors. Experimental results are reported for two different d4-benzenes. © 1991.
引用
收藏
页码:254 / 260
页数:7
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