EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM HIGHLY CONTAMINATED SOILS - A COMPARISON BETWEEN SOXHLET, MICROWAVE AND SUPERCRITICAL-FLUID EXTRACTION TECHNIQUES

被引：46

作者：

DEAN, JR ^{[1
]}

BARNABAS, IJ ^{[1
]}

FOWLIS, IA ^{[1
]}

机构：

[1] NORTHUMBRIA UNIV,DEPT CHEM & LIFE SCI,NEWCASTLE TYNE NE1 8ST,TYNE & WEAR,ENGLAND

来源：

ANALYTICAL PROCEEDINGS | 1995年 / 32卷 / 08期

关键词：

D O I：

10.1039/ai9953200305

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A direct comparison between Soxhlet, microwave-assisted extraction and supercritical fluid extraction is made. Each technique was used to extract sixteen polycyclic aromatic hydrocarbons (PAHs) from a native, contaminated soil. The total amounts of PAHs found were 297.4, 422.9 and 458.0 mg kg(-1) using Soxhlet, microwave-assisted extraction and supercritical fluid extraction. The merits and disadvantages of each extraction technique is discussed.

引用

页码：305 / 308

页数：4

共 5 条

[1] SUPERCRITICAL-FLUID EXTRACTION OF ANALYTES FROM ENVIRONMENTAL-SAMPLES - A REVIEW
BARNABAS, IJ
DEAN, JR
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[J]. ANALYST, 1994, 119 (11) : 2381 - 2394
[2] SELECTIVE SUPERCRITICAL-FLUID EXTRACTION OF ORGANOCHLORINE PESTICIDES AND HERBICIDES FROM AQUEOUS SAMPLES
BARNABAS, IJ
DEAN, JR
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OWEN, SP
[J]. JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1994, 32 (12) : 547 - 551
[3] EXTRACTION OF POLYCYCLIC AROMATIC-HYDROCARBONS FROM HIGHLY CONTAMINATED SOILS USING MICROWAVE-ENERGY
BARNABAS, IJ
DEAN, JR
FOWLIS, IA
OWEN, SP
[J]. ANALYST, 1995, 120 (07) : 1897 - 1904
[4] BARNABAS IJ, IN PRESS ANAL CHEM
[5] 1986, US EPA8100 METH

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