SOL-GEL SYNTHESIS OF BARIUM-TITANATE USING BARIUM CARBONATE WITH GLACIAL ACETIC-ACID AND BUTYL TITANATE MONOMER

被引：8

作者：

GODBOLE, PD

DESHPANDE, SB

POTDAR, HS

DATE, SK

机构：

[1] Physical Chemistry Division, National Chemical Laboratory, Pune

来源：

MATERIALS LETTERS | 1991年 / 12卷 / 1-2期

关键词：

D O I：

10.1016/0167-577X(91)90065-E

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Barium carbonate with glacial acetic acid and butyl titanate monomer (BTM) were used as Ba and Ti precursors to obtain sols and hard transparent gels at room temperature. After the calcination of the gels at various temperatures (25-1250-degrees-C) in air, the mixed Ba/Ti powder was characterized by DTA/DTG/TG, XRD and IR. The formation of tetragonal BaTiO3 as a major phase was seen to occur around 550-degrees-C.

引用

页码：97 / 101

页数：5

共 11 条

[1] AN AQUEOUS SYNTHESIS OF BARIUM TITANATE
FLASCHEN, SS
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1955, 77 (23) : 6194 - 6194
[2] SOL-GEL SYNTHESIS OF ULTRAFINE BARIUM-TITANATE USING BUTYL TITANATE MONOMER AND BARIUM NITRATE AND ITS CHARACTERIZATION
GODBOLE, PD
DESHPANDE, SB
DATE, SK
NAWATHEY, R
OGALE, SB
[J]. FERROELECTRICS, 1990, 102 : 91 - 97
[3] HENCH LL, 1986, SCI CERAMIC CHEM PRO
[4] KULCSAR F, 1956, J AM CERAM SOC, V39, P13
[5] OZAKI Y, 1988, ADV CERAM, P165
[6] LOW-TEMPERATURE SYNTHESIS AND DIELECTRIC-PROPERTIES OF CERAMICS DERIVED FROM AMORPHOUS BARIUM-TITANATE GELS AND CRYSTALLINE POWDERS
PHULE, PP
RISBUD, SH
[J]. MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 1989, 3 (03): : 241 - 247
[7] PHULE PP, 1988, ADV CERAM MATER, V3, P183
[8] LOW-TEMPERATURE SYNTHESIS OF ULTRAFINE BARIUM-TITANATE (BATIO3) USING ORGANOMETALLIC BARIUM AND TITANIUM PRECURSORS
POTDAR, HS
SINGH, P
DESHPANDE, SB
GODBOLE, PD
DATE, SK
[J]. MATERIALS LETTERS, 1990, 10 (03) : 112 - 117
[9] SYNTHESIS OF GLASS PRECURSOR BAO,TIO2,NH2OBY GEL PROCESSING
REHSPRINGER, JL
POIX, P
BERNIER, JC
[J]. JOURNAL OF NON-CRYSTALLINE SOLIDS, 1986, 82 (1-3) : 286 - 292
[10] REHSPRINGER JL, 1988, ULTRASTRUCTURE PROCE, P925

← 1 2 →