ANALYSIS OF OCHRATOXINS FROM BUFFERED RUMEN FLUID BY REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY (HPLC)

被引:15
作者
LERCH, CM [1 ]
MULLER, HM [1 ]
机构
[1] UNIV HOHENHEIM,INST ANIM NUTR,EMIL WOLFF STR 10,W-7000 STUTTGART 70,GERMANY
关键词
Column liquid chromatography; Mycotoxins; Ochratoxin A; Rumen fluid;
D O I
10.1007/BF02328510
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
An efficient procedure for the extraction and analysis of ochratoxins A, B, C and α from buffered rumen fluid has been developed. The samples have been cleaned up byliquid-liquid extraction and the separation of chratoxins was by isocratic elution on a 5μm C18 ODS-column which 0.083 M phosphoric acid/acetonitrile/isopropanol (55/35/10). © 1990 Friedr. Vieweg & Sohn Verlagsgesellschaft mbH.
引用
收藏
页码:424 / 427
页数:4
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