DETERMINATION OF LEAD IN SOIL BY SLURRY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY WITH A FAST TEMPERATURE PROGRAM

被引:30
作者
HINDS, MW
LATIMER, KE
JACKSON, KW
机构
[1] UNIV SASKATCHEWAN,DEPT CHEM,SASKATOON S7N 0W0,SASKATCHEWAN,CANADA
[2] SUNY ALBANY,NEW YORK STATE DEPT HLTH,WADSWORTH CTR LABS,ALBANY,NY 12201
[3] SUNY ALBANY,SCH PUBL HLTH,ALBANY,NY 12201
关键词
ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY; SLURRY; FAST TEMPERATURE PROGRAM; SOIL ANALYSIS;
D O I
10.1039/ja9910600473
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A fast temperature programme for the determination of Pb in soil by slurry-electrothermal atomic absorption spectrometry was developed by omitting the charring step and drying at a higher temperature for a shorter time. The effects of drying temperature and time were systematically studied. Work with phosphate and Mg-Pd as chemical modifiers indicates that better results can be obtained without the use of modifiers.
引用
收藏
页码:473 / 476
页数:4
相关论文
共 23 条
[1]   FAST-RESPONSE SYSTEM FOR SIGNAL ACQUISITION AND PROCESSING IN ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY [J].
ALLEN, E ;
JACKSON, KW .
ANALYTICA CHIMICA ACTA, 1987, 192 (02) :355-359
[2]   MASS-SPECTRAL INVESTIGATION OF MECHANISMS OF LEAD VAPORIZATION FROM A GRAPHITE SURFACE USED IN ELECTROTHERMAL ATOMIZERS [J].
BASS, DA ;
HOLCOMBE, JA .
ANALYTICAL CHEMISTRY, 1987, 59 (07) :974-980
[3]  
BENDICHO C, 1990, SPECTROCHIM ACTA B, V45, P6769
[4]   RAPID SLURRY ANALYSIS OF SOLID COAL AND FLY-ASH SAMPLES [J].
BRADSHAW, D ;
SLAVIN, W .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1989, 44 (12) :1245-1256
[5]  
CZOBIK EJ, 1977, TALANTA, V24, P837
[6]   TIME-DEPENDENT TEMPERATURE DISTRIBUTION OF GRAPHITE-TUBE ATOMIZERS [J].
FALK, H ;
GLISMANN, A ;
BERGANN, L ;
MINKWITZ, G ;
SCHUBERT, M ;
SKOLE, J .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1985, 40 (03) :533-542
[7]   DETERMINATION OF ALUMINUM IN DIALYSATE FLUIDS BY ATOMIC-ABSORPTION SPECTROMETRY WITH ELECTROTHERMAL ATOMIZATION [J].
HALLS, DJ ;
FELL, GS .
ANALYST, 1985, 110 (03) :243-246
[8]   DIRECT DETERMINATION OF CADMIUM IN URINE BY ELECTROTHERMAL ATOMIZATION ATOMIC-ABSORPTION SPECTROMETRY [J].
HALLS, DJ ;
BLACK, MM ;
FELL, GS ;
OTTAWAY, JM .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1987, 2 (03) :305-309
[9]   APPLICATION OF RAPID FURNACE PROGRAMS IN ATOMIC-ABSORPTION SPECTROMETRY TO THE DETERMINATION OF LEAD, CHROMIUM AND COPPER IN DIGESTS OF PLANT MATERIALS [J].
HALLS, DJ ;
MOHL, C ;
STOEPPLER, M .
ANALYST, 1987, 112 (02) :185-189
[10]   SPEEDING UP DETERMINATIONS BY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY [J].
HALLS, DJ .
ANALYST, 1984, 109 (08) :1081-1084