PREPARATION AND CHARACTERIZATION OF CRYSTALLINE N-ACYLAMMONIUM SALTS

被引：50

作者：

KING, JA

BRYANT, GL

机构：

[1] General Electric Company, Corporate Research and Development, Schenectady, New York 12301

来源：

JOURNAL OF ORGANIC CHEMISTRY | 1992年 / 57卷 / 19期

关键词：

D O I：

10.1021/jo00045a025

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The reaction of a tertiary amine with an acid chloride or chloroformate followed by anion exchange with either sodium tetraphenylborate or silver tetrafluoroborate provides stable, nonhygroscopic, crystalline acylammonium salts.

引用

页码：5136 / 5139

页数：4

共 50 条

[1] KINETICS OF HYDROLYSIS AND AMINOLYSIS OF 1-METHOXYCARBONYLPYRIDINIUM IONS [J].

BATTYE, PJ ;

IHSAN, EM ;

MOODIE, RB .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1980, (05) :741-748

[2] MECHANISMS OF CATALYSIS OF NUCLEOPHILIC REACTIONS OF CARBOXYLIC ACID DERIVATIVES [J].

BENDER, ML .

CHEMICAL REVIEWS, 1960, 60 (01) :53-113

[3]

BUNTING JW, 1984, ADV HETEROCYCL CHEM, V2, P165

[4] THE MILD AND SELECTIVE N-DEBENZYLATION OF TERTIARY ALKYLAMINES USING BETA-TRIMETHYLSILYLETHYL CHLOROFORMATE [J].

CAMPBELL, AL ;

PILIPAUSKAS, DR ;

KHANNA, IK ;

RHODES, RA .

TETRAHEDRON LETTERS, 1987, 28 (21) :2331-2334

[5] KINETICS AND MECHANISM OF THE REACTIONS OF 2,4-DINITROPHENYL ACETATE WITH SECONDARY ALICYCLIC AMINES - DIFFERENT NUCLEOFUGALITIES OF ALICYCLIC AMINES AND PYRIDINES FROM A TETRAHEDRAL INTERMEDIATE [J].

CASTRO, EA ;

URETA, C .

JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (05) :1676-1679

[6] SOLVENT EFFECT ON THE RELATIVE NUCLEOFUGALITIES OF PYRIDINES AND PHENOXIDE IONS - BRONSTED-TYPE PLOTS IN THE PYRIDINOLYSIS OF 2,4-DINITROPHENYL METHYL CARBONATE AND 2,4-DINITROPHENYL ACETATE IN AQUEOUS ETHANOL [J].

CASTRO, EA ;

BORQUEZ, MT ;

PARADA, PM .

JOURNAL OF ORGANIC CHEMISTRY, 1986, 51 (26) :5072-5077

[7]

CASTRO EA, 1987, J CHEM RES-S, P358

[8] CHOLESTERYL CHLOROFORMATE [J].

CHANDROSS, RJ ;

BORDNER, J .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1978, 34 (SEP) :2872-2875

[9] A SINGLE TRANSITION-STATE IN THE TRANSFER OF THE METHOXYCARBONYL GROUP BETWEEN ISOQUINOLINE AND SUBSTITUTED PYRIDINES IN AQUEOUS-SOLUTION [J].

CHRYSTIUK, E ;

WILLIAMS, A .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1987, 109 (10) :3040-3046

[10] REGIOSELECTIVE ADDITION OF NUCLEOPHILES TO 1-(PHENOXYCARBONYL)-3-TRIALKYLSTANNYLPYRIDINIUM SALTS [J].

COMINS, DL ;

MANTLO, NB .

TETRAHEDRON LETTERS, 1987, 28 (07) :759-762

← 1 2 3 4 5 →