DETERMINATION OF TETRAMINE IN POSTMORTEM SPECIMENS BY GC-NPD

被引:9
作者
JING, S
YU, ZS
ZHAO, LZ
ZHOU, HZ
机构
[1] Institute of Forensic Science, Ministry of Public Security, Beijing
关键词
D O I
10.1093/jat/18.5.275
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for the determination of tetramine in postmortem specimens is reported. Tetramine is an organosulfur rodenticide. Parathion, an organophosphorous insecticide, was adopted as the internal standard. Both were extracted from biological materials by benzene and purified by an aluminum oxide column. The extract was analyzed by a gas chromatograph equipped with a nitrogen-phosphorous detector. The extraction efficiency was greater than 90%, and the limit of detection was 0.05 μg/g for the liver. The standard curve was linear in the range 0.5-50 μg/g for the liver, and the correlation coefficient was equal to 0.9993. © 1994, Oxford University Press.
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页码:275 / 277
页数:3
相关论文
共 3 条
[2]  
Hecht G., 1953, United States patent, Patent No. [2,650,186, 2650186]
[3]  
ZHONG JH, 1990, 4TH SEM FOR SCI TECH