CHARACTERIZATION OF ALUMINA POWDER USING MULTIPLE SMALL-ANGLE NEUTRON-SCATTERING .2. EXPERIMENT

被引:27
作者
HARDMANRHYNE, KA
BERK, NF
机构
[1] NBS, Inst for Materials Science, & Engineering, Gaithersburg, MD,, USA, NBS, Inst for Materials Science & Engineering, Gaithersburg, MD, USA
关键词
LASER BEAMS - Scattering - MICROSCOPES; ELECTRON - Applications - NEUTRONS - Scattering - PARTICLE SIZE ANALYSIS - POWDERS;
D O I
10.1107/S0021889885010731
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Small-angle neutron scattering techniques developed in the preceding paper are used to obtain microstructural parameters of high-purity alumina powder. The values of the particle size, volume fraction and surface area have been obtained and are compared to data from techniques such as laser light scattering, X-ray sedigraph and scanning electron microscopy. The particles exhibit a log-normal distribution and are spherical in shape with a mean particle size of 342 nm determined from SANS analyses of both beam broadening and Porod regions.
引用
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页码:473 / 479
页数:7
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