AN EASY ROUTE TO SYNTHESIZE 1,5-ARYLODIAZEPIN-2-ONES

被引：60

作者：

BOUGRIN, K ^{[1
]}

BENNANI, AK ^{[1
]}

TETOUANI, SF ^{[1
]}

SOUFIAOUI, M ^{[1
]}

机构：

[1] UNIV MOHAMMED 5,FAC SCI,CHIM PLANTES & SYNTH ORGAN & BIOORGAN LAB,RABAT,MOROCCO

来源：

TETRAHEDRON LETTERS | 1994年 / 35卷 / 45期

关键词：

CONDENSATION; MICROWAVE; 1,5-ARYLODIAZEPIN-2-ONES;

D O I：

10.1016/S0040-4039(00)74410-8

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A series of 1,5-arylodiazepin-2-ones is prepared by the condensation of the appropriate o-beta-arylenediamines with beta-ketoesters in xylene under microwave irradiation. The reaction time is shortened to 10 mn, and the products are obtained in high yields. No by products are observed. Specific effects of microwaves are evidenced as no reaction occurs by classical heating in the same conditions.

引用

页码：8373 / 8376

页数：4

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