THE USE OF SODIUM TETRAETHYLBORATE FOR THE DERIVATIZATION AND ANALYSIS OF SELENIUM CONTAINING COMPOUNDS

被引：37

作者：

CLARK, S ^{[1
]}

CRAIG, PJ ^{[1
]}

机构：

[1] DE MONTFORT UNIV,DEPT CHEM,GATEWAY,POB 143,LEICESTER LE1 9BH,ENGLAND

来源：

MIKROCHIMICA ACTA | 1992年 / 109卷 / 1-4期

关键词：

SODIUM TETRAETHYLBORATE; ETHYLATION; ANALYSIS; SELENIUM;

D O I：

10.1007/BF01243227

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Several selenium containing compounds have been derivatized to diethyl selenide using sodium tetraethylborate. The evolved diethyl selenide was detected by gas chromatography interfaced with atomic absorption or mass spectroscopic methods. Derivatization was carried out on the analyte in a sealed vial using an aqueous solution of sodium tetraethylborate (2%) added by means of a syringe.

引用

页码：141 / 144

页数：4

共 15 条

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