DETERMINATION OF INORGANIC ARSENIC AND METHYLARSENIC COMPOUNDS BY GAS-CHROMATOGRAPHY AND MULTIPLE ION DETECTION MASS-SPECTROMETRY AFTER HYDRIDE GENERATION HEPTANE COLD TRAP

被引:44
作者
ODANAKA, Y
TSUCHIYA, N
MATANO, O
GOTO, S
机构
[1] Inst. Environ. Toxicol., Kodaira-shi, Tokyo 187, Japan
关键词
CHROMATOGRAPHIC ANALYSIS - FUNGICIDES - HERBICIDES - MASS SPECTROMETERS - PESTICIDES;
D O I
10.1021/ac00257a025
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The limit of detection for 50-mL sample was 0. 2-0. 4 ng mL** minus **1 of arsenic for arsenic compounds. Relative standard deviations ranged from 2% to 5% for distilled water replicates spiked at the 10 ppb level. Recoveries of all four arsenic species from soil and plant extracts, urine, and river water ranged from 85% to 100%.
引用
收藏
页码:929 / 932
页数:4
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