SYNTHESIS OF THE C-14-LABELED JUVENOID W328

被引：2

作者：

ELBERT, T

HAVLICEK, L

WIMMER, Z

BUBNER, M

机构：

[1] UEB AVCR,CR-14220 PRAGUE 4,CZECH REPUBLIC

[2] UOCHB AVCR,CR-16610 PRAGUE 6,CZECH REPUBLIC

[3] FORSCH ZENTRUM ROSSENDORF EV,INST RADIOCHEM,O-8051 DRESDEN,GERMANY

来源：

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 1994年 / 34卷 / 04期

关键词：

C-14 LABELED JUVENOID W 328; P-HYDROXY(RING-U-C-14) BENZOIC ACID; (14)C-LABELED PESTICIDE;

D O I：

10.1002/jlcr.2580340409

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The labelled juvenoid 2-(4-(2-(ethoxycarbamatoethoxy) (benzene-U-C-14) benzyl)-1-cyclohexanone ethylene acetal (8) (W 328) was prepared starting from p-hydroxy(ring-U-C-14) benzoic acid (1) by a seven step synthesis in 11% overall yield. The reaction conditions previously reported for the ''cold'' synthesis of the W 328 (B) were modified to suit the small scale preparation.

引用

页码：377 / 382

页数：6

共 6 条

[1]

ELBERT T, IN PRESS COLL CZECH

[2]

ELLAMES GJ, 1991, J LABEL COMP RADIOPH, V20, P29

[3]

MATUCHA M, UNPUB

[4] A NEW METHOD OF PREPARATION OF DIAZOMETHANE [J].