METHODS AND APPARATUS FOR IN-SITU INVESTIGATIONS WITH THE SCANNING FORCE MICROSCOPE

被引:17
作者
KIPP, S [1 ]
LACMANN, R [1 ]
SCHNEEWEISS, MA [1 ]
机构
[1] TECH UNIV CAROLO WILHELMINA BRAUNSCHWEIG,INST PHYS & THEORET CHEM,HANS SOMMER STR 10,D-38106 BRAUNSCHWEIG,GERMANY
关键词
D O I
10.1016/0022-0248(94)90122-8
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Various methods of carrying out time resolved in situ monitoring of crystallization processes with the scanning force microscope (SFM) were tested and improved. First investigations, taking place in static liquids, were performed in a simple cup sample holder and in the liquid cell supplied by the manufacturers of the SFM. Continuous flow conditions were, realized with a new recirculating flow system, which in addition allows temperature control. The different apparative approaches were tested with lab-grown crystals of L-ascorbic acid and lithium fluoride, as well as freshly cleaved fragments of the naturally occurring mineral calcite.
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页码:291 / 298
页数:8
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