MEASUREMENT OF PLATINUM IN BIOMEDICAL SILICONES BY ICP-MS

被引:15
作者
ELJAMMAL, A [1 ]
TEMPLETON, DM [1 ]
机构
[1] UNIV TORONTO,DEPT CLIN BIOCHEM,TORONTO,ON M5G 1L5,CANADA
来源
ANALYTICAL PROCEEDINGS | 1995年 / 32卷 / 08期
关键词
D O I
10.1039/ai9953200293
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method is described for processing organosilicone oils and gels for introduction by nebulization into an ICP-MS. A silicone oil sample was free of detectable contamination with trace elements. Platinum, added as a catalyst during manufacture, was found to be present at approximately 4.5 mu g g(-1) in a silicone breast implant. No other trace elements were present in significant quantities in the implant. Quantitative recovery of Pt from silicone gel was achieved by dispersion in aqua regia, extraction of the organosilicone with diethyl ether, and back-extraction with acid.
引用
收藏
页码:293 / 295
页数:3
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