STUDIES ON ISOCYANIDES AND RELATED-COMPOUNDS - INVESTIGATION ON THE REACTION BETWEEN (Z)-ALKYL 3-DIMETHYLAMINO-2-ISOCYANOACRYLATES AND ACYL CHLORIDES

被引：6

作者：

BOSSIO, R

MARCACCINI, S

PEPINO, R

PAOLI, P

POLO, C

机构：

[1] UNIV FLORENCE,DIPARTIMENTO ENERGET,I-50139 FLORENCE,ITALY

[2] UNIV EXTREMADURA,FAC VET,DEPT QUIM ORGAN,E-10071 CACERES,SPAIN

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1993年 / 30卷 / 02期

关键词：

D O I：

10.1002/jhet.5570300256

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The reaction between (Z)-methyl 3-dimethylamino-2-isocyanoacrylate (1a) and acyl chlorides 2a,b did not afford methyl 2-acyl-1-methyl-1H-imidazole-4-carboxylates 3a,b, as previously reported, but 2-acyl-4-dimeth-ylaminomethyleneoxazol-5(4H)-ones 4a,b.

引用

页码：575 / 577

页数：3

共 10 条

[1]

[Anonymous], 1974, INT TABLES XRAY CRYS, VIV

[2]

BOSSIO R, IN PRESS J CHEM RE S

[3] SIR88 - A DIRECT-METHODS PROGRAM FOR THE AUTOMATIC SOLUTION OF CRYSTAL-STRUCTURES [J].

BURLA, MC ;

CAMALLI, M ;

CASCARANO, G ;

GIACOVAZZO, C ;

POLIDORI, G ;

SPAGNA, R ;

VITERBO, D .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1989, 22 :389-393

[4]

HOFMANN P, 1970, CHEM CYANO GROUP, P860

[5]

JOHNSON CK, 1971, ORNL3794

[6]

KUHLE E, 1973, CHEM SULFENIC ACIDS, P57

[7]

LAU HH, 1982, LIEBIGS ANN CHEM, P2093

[8]

SHELDRICK GM, 1976, SHELX PROGRAM CRYSTA

[9] ISONITRILE .3. DIE ADDITION VON CARBONSAURECHLORIDEN AN ISONITRILE [J].

UGI, I ;

FETZER, U .

CHEMISCHE BERICHTE-RECUEIL, 1961, 94 (04) :1116-1121

[10] AN EMPIRICAL-METHOD FOR CORRECTING DIFFRACTOMETER DATA FOR ABSORPTION EFFECTS [J].

WALKER, N ;

STUART, D .

ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (JAN) :158-166

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