BIS(TRIMETHYLSILYL)PHOSPHIDOMETAL COMPLEXES .1. ISOLATION AND NMR-SPECTRA OF LI4(MU-2-PSIME32)2(M-3-PSIME32)2(THF)2 (I), LI(PSIME32)(PMDETA) (II), AND X-RAY STRUCTURES OF COMPOUND I AND [LI(MU-PSIME32)(THF)2]2 (III)

被引：81

作者：

HEY, E

HITCHCOCK, PB

LAPPERT, MF

RAI, AK

机构：

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1987年 / 325卷 / 1-2期

关键词：

D O I：

10.1016/0022-328X(87)80382-0

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

引用

页码：1 / 12

页数：12

共 29 条

[1] LOWER COORDINATED PHOSPHORUS-COMPOUNDS .50. A STABLE 1,2,4-THIADIPHOSPHOLE (2,4-DIPHOSPHATHIOPHENE) [J].

APPEL, R ;

MOORS, R .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1986, 25 (06) :567-567

[2] THE LADDERING PRINCIPLE IN LITHIUM AMIDE CHEMISTRY - THE CRYSTAL AND MOLECULAR-STRUCTURE OF THE PYRROLIDIDOLITHIUM ADDUCT [H2C(CH2)3NLI]3.MEN(CH2CH2NME2)2 [J].

ARMSTRONG, DR ;

BARR, D ;

CLEGG, W ;

MULVEY, RE ;

REED, D ;

SNAITH, R ;

WADE, K .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1986, (11) :869-870

[3] THE 1ST X-RAY CRYSTAL STRUCTURAL CHARACTERIZATIONS OF ALKALI-METAL ALKYL THIOLATES - X-RAY CRYSTAL-STRUCTURES OF [LI2(THF)4(SCH(SIME3)2)2] AND [LI2(THF)3.5(SC(SIME3)3)2] (THF = TETRAHYDROFURAN) [J].

ASLAM, M ;

BARTLETT, RA ;

BLOCK, E ;

OLMSTEAD, MM ;

POWER, PP ;

SIGEL, GE .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1985, (23) :1674-1675

[4] MOLECULAR-STRUCTURES OF BIS(TRIMETHYLSILYL)METHYL-LITHIUM [(LIR)N, R=CH(SIME3)2] IN THE VAPOR (GAS-PHASE ELECTRON-DIFFRACTION - A MONOMER, N=1) AND THE CRYSTAL (X-RAY - A POLYMER, N= INFINITY) [J].

ATWOOD, JL ;

FJELDBERG, T ;

LAPPERT, MF ;

LUONGTHI, NT ;

SHAKIR, R ;

THORNE, AJ .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (17) :1163-1165

[5] STRUCTURAL CHARACTERIZATION OF THE SOLVATE COMPLEXES OF THE LITHIUM DIORGANOPHOSPHIDES [(LI(ET2O)PPH2)-INFINITY], [(LI(THF)2PPH2)-INFINITY], AND [(LI(THF)P(C6H11)2)-INFINITY] [J].

BARTLETT, RA ;

OLMSTEAD, MM ;

POWER, PP .

INORGANIC CHEMISTRY, 1986, 25 (08) :1243-1247

[6] OBSERVATION ON A SIMPLE METHOD OF PREPARING TRIS(TRIMETHYLSILYL)PHOSPHINE [J].

BECKER, G ;

HOLDERICH, W .

CHEMISCHE BERICHTE-RECUEIL, 1975, 108 (07) :2484-2485

[7] TRIMETHYLSILYL DERIVATIVES OF VB-ELEMENTS .4. SYNTHESIS AND STRUCTURE OF LITHIUM BIS(TRIMETHYLSILYL)ANTIMONIDE . DME [J].

BECKER, G ;

MUNCH, A ;

WITTHAUER, C .

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1982, 492 (09) :15-27

[8] TRIMETHYLSILYL DERIVATIVES OF VB-ELEMENTS .5. MOLECULAR AND CRYSTAL-STRUCTURE OF LITHIUM BIS(TRIMETHYLSILYL)ARSENIDE . DME [J].

BECKER, G ;

WITTHAUER, C .

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1982, 492 (09) :28-36

[9] LITHIUM AND SODIUM 2,6-DI-TERT-BUTYLPHENOXIDES AND THE CRYSTAL AND MOLECULAR-STRUCTURE OF [LI(OC6H2ME-4-BUT2-2,6)(OET2)]2 [J].

CETINKAYA, B ;

GUMRUKCU, I ;

LAPPERT, MF ;

ATWOOD, JL ;

SHAKIR, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1980, 102 (06) :2086-2088

[10] CRYSTAL-STRUCTURE OF DIMERIC N-LITHIOHEXAMETHYLDISILAZANE ETHERATE, [(ET2O)LI[MU-N(SIME3)2]2LI(OET2)] [J].

ENGELHARDT, LM ;

MAY, AS ;

RASTON, CL ;

WHITE, AH .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1983, (08) :1671-1673

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