GENERATION OF SPIT-FLOW MICRO-GRADIENTS FOR CAPILLARY HPLC

被引：28

作者：

BERLONI, A ^{[1
]}

CAPPIELLO, A ^{[1
]}

FAMIGLINI, G ^{[1
]}

PALMA, P ^{[1
]}

机构：

[1] UNIV URBINO,IST SCI CHIM,I-61029 URBINO,ITALY

来源：

CHROMATOGRAPHIA | 1994年 / 39卷 / 5-6期

关键词：

COLUMN LIQUID CHROMATOGRAPHY; CAPILLARY COLUMNS FOR LC; MICRO-GRADIENT GENERATION;

D O I：

10.1007/BF02274514

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The generation of a micro-gradient for micro HPLC capillary columns is described. The system used is a modified and improved version of a split flow gradient elution device. Gradient tests have been performed and have shown good reproducibility under all conditions. The system has been successfully coupled with a particle beam LC-MS interface and the analysis of a mixture of twenty seven basic or neutral pesticides is reported.

引用

页码：279 / 284

页数：6

共 13 条

[1] BANKS JF, 1990, J MICROCOLUMN SEP, V2, P84
[2] A SIMPLE HIGHLY REPRODUCIBLE GRADIENT SYSTEM FOR MICRO COLUMN HPLC
BAUER, H
[J]. CHROMATOGRAPHIA, 1989, 28 (5-6) : 289 - 292
[3] MICRO-HPLC 1 - LINEAR BREAKTHROUGH-GRADIENTS USING THE DISCONTINUOUS INTERFACE BETWEEN ELUENTS IN A PACKED GRADIENT-GENERATOR COLUMN
BERRY, V
ISHII, D
TAKEUCHI, T
[J]. JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1985, 8 (10): : 659 - 664
[4] NEW MATERIALS AND PACKING TECHNIQUES FOR MICRO-HPLC PACKED CAPILLARY COLUMNS
CAPPIELLO, A
PALMA, P
MANGANI, F
[J]. CHROMATOGRAPHIA, 1991, 32 (7-8) : 389 - 391
[5] MICRO FLOW-RATE PARTICLE BEAM INTERFACE FOR CAPILLARY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY
CAPPIELLO, A
BRUNER, F
[J]. ANALYTICAL CHEMISTRY, 1993, 65 (09) : 1281 - 1287
[6] EFFICIENT INTRODUCTION OF HPLC FRACTIONS INTO A HIGH-PERFORMANCE TANDEM MASS-SPECTROMETER
CAPPIELLO, A
PALMA, P
PAPAYANNOPOULOS, IA
BIEMANN, K
[J]. CHROMATOGRAPHIA, 1990, 30 (9-10) : 477 - 483
[7] A MINIATURE GRADIENT ELUTION SYSTEM FOR LIQUID-CHROMATOGRAPHY WITH PACKED CAPILLARY COLUMNS
KARLSSON, KE
NOVOTNY, M
[J]. JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1984, 7 (07): : 411 - 413
[8] PALMA P, 1992, ANN CHIM-ROME, V82, P371
[9] STEPWISE GRADIENT ELUTION USING SWITCHING VALVES IN MICRO HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
TAKEUCHI, T
NIWA, T
ISHII, D
[J]. JOURNAL OF CHROMATOGRAPHY, 1987, 405 : 117 - 124
[10] CONTINUOUS GRADIENT ELUTION IN MICRO HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
TAKEUCHI, T
ISHII, D
[J]. JOURNAL OF CHROMATOGRAPHY, 1982, 253 (01): : 41 - 47

← 1 2 →