THE DETERMINATION OF ABAMECTIN FROM SOIL AND ANIMAL TISSUE BY SUPERCRITICAL-FLUID EXTRACTION AND FLUORESCENCE DETECTION

被引:19
作者
BROOKS, MW [1 ]
UDEN, PC [1 ]
机构
[1] UNIV MASSACHUSETTS,DEPT CHEM,AMHERST,MA 01003
来源
PESTICIDE SCIENCE | 1995年 / 43卷 / 02期
关键词
ABAMECTIN; SFE; HPLC; FLUORESCENCE DETECTION; EXTRACTION;
D O I
10.1002/ps.2780430207
中图分类号
S3 [农学(农艺学)];
学科分类号
0901 ;
摘要
The insecticide abamectin is extracted from soil and animal tissue by supercritical fluid extraction. Supercritical carbon dioxide modified with 9% 2-methoxyethanol extracted abamectin from soil samples at levels up to 11 ng g-1 with greater than 80% efficiency. Recovery at fortification levels of 5 ng g-1 were obtainable without the need for clean-up. Abamectin was also easily extracted from animal tissue at levels of 22 ng g-1 without interfering coextractives. Extracted abamectin was determined by liquid chromatography of a fluorescent derivative.
引用
收藏
页码:141 / 146
页数:6
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