NEW DIRECT IODINATION OF TETRATHIAFULVALENE (TTF) - MONO-IODO-TTF AND DI-IODO-TTF AND THEIR X-RAY CRYSTAL-STRUCTURES

被引：54

作者：

WANG, CS ^{[1
]}

ELLERN, A ^{[1
]}

KHODORKOVSKY, V ^{[1
]}

BERNSTEIN, J ^{[1
]}

BECKER, JY ^{[1
]}

机构：

[1] BEN GURION UNIV NEGEV,DEPT CHEM,IL-84120 BEER SHEVA,ISRAEL

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1994年 / 08期

关键词：

D O I：

10.1039/c39940000983

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

2-lodo-(1) and 2,6(7)-diiodo-tetrathiafulvalenes (2a, 2b) have been synthesized in good yields, by treating the corresponding lithiated intermediates of TTF with perfluorohexyl iodide; the X-ray crystal structures of 1 and 2a have been determined.

引用

页码：983 / 984

页数：2

共 8 条

[1] PREPARATION OF MONO-BROMOTETRATHIAFULVALENES AND 1,2-DI-BROMOTETRATHIAFULVALENES (TTFBR AND 1,2-TTFBR2)
BECKER, JY
BERNSTEIN, J
BITTNER, S
SHAHAL, L
SHAIK, SS
[J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1991, (02) : 92 - 93
[2] BRYCE MR, 1991, SYNTHESIS-STUTTGART, P263
[3] GENERAL-METHOD FOR THE PREPARATION OF SUBSTITUTED TETRATHIAFULVALENES AND DIRECTING EFFECTS OF SUBSTITUENTS
GREEN, DC
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1979, 44 (09) : 1476 - 1479
[4] JORGENSEN M, 1989, SYNTHESIS-STUTTGART, P207
[5] KHODORKOVSKY V, 1989, J MOL ELECTRON, V5, P33
[6] KREITSBERGA YN, 1989, ZH ORG KHIM+, V25, P1456
[7] NAKAYAMA J, 1986, HETEROCYCLES, V24, P1145, DOI 10.3987/R-1986-04-1145
[8] PROTON ACTIVITY OF 1,3-DITHIOLIUM SYSTEM
PRINZBAC.H
BERGER, H
LUTTRING.A
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1965, 4 (05) : 435 - &

← 1 →