NEW CHIRAL POLYAMIDE STATIONARY PHASES FOR CHROMATOGRAPHIC ENANTIOMER SEPARATION

被引：27

作者：

ARLT, D ^{[1
]}

BOMER, B ^{[1
]}

GROSSER, R ^{[1
]}

LANGE, W ^{[1
]}

机构：

[1] BAYER AG,CENT RES & DEV,BLDG Q18,W-5090 LEVERKUSEN,GERMANY

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH | 1991年 / 30卷 / 12期

关键词：

D O I：

10.1002/anie.199116621

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The diastereomeric polyamides 1 and 2 furnish stationary phases for enantiomeric separations with high enantiostereoselectivity. These methacryloylamides can be obtained in good yield in kg quantities and can be polymerized on stationary phases as well as transformed into crosslinked bead polymers for use in preparative separations.

引用

页码：1662 / 1664

页数：3

共 17 条

[1] CHROMATOGRAPHIC-SEPARATION OF ENANTIOMERS .15. ENANTIOMERIC RESOLUTION BY HPLC ON SILICA-GEL-BOUND, OPTICALLY-ACTIVE POLYAMIDES [J].

BLASCHKE, G ;

BROKER, W ;

FRAENKEL, W .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1986, 25 (09) :830-831

[2] INVESTIGATION OF CHROMATOGRAPHIC RESOLUTIONS OF RACEMATES, .6. POLYMERIC AMINO-ACID DERIVATIVES AS OPTICALLY-ACTIVE ADSORBENTS [J].

BLASCHKE, G ;

SCHWANGHART, AD .

CHEMISCHE BERICHTE-RECUEIL, 1976, 109 (06) :1967-1975

[3]

BLASCHKE G, 1988, CHROMATOGRAPHIC CHIR, V40, P179

[4]

Blaschke G., 1986, ANGEW CHEM, V98, P808

[5]

BOMER B, 1988, Patent No. 282770

[6] POLYMER ENCAPSULATED STATIONARY PHASES - ADVANTAGES, PROPERTIES AND SELECTIVITIES [J].

ENGELHARDT, H ;

LOW, H ;

EBERHARDT, W ;

MAUSS, M .

CHROMATOGRAPHIA, 1989, 27 (11-12) :535-543

[7] BENZOYL CELLULOSE BEADS IN THE PURE POLYMERIC FORM AS A NEW POWERFUL SORBENT FOR THE CHROMATOGRAPHIC RESOLUTION OF RACEMATES [J].

FRANCOTTE, E ;

WOLF, RM .

CHIRALITY, 1991, 3 (01) :43-55

[8]

GERLACH U, 1989, LIEBIGS ANN CHEM, P103

[9] CHROMATOGRAPHIC RESOLUTION, CIRCULAR-DICHROISM SPECTRA, AND ABSOLUTE-CONFIGURATIONS OF DIMERS OF 5H-INDOLO[1,7-AB][1]BENZAZEPINE AND COUMARIN WITH C2 SYMMETRY [J].

HALLBERG, A ;

ISAKSSON, R ;

MARTIN, AR ;

SANDSTROM, J .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (12) :4387-4392

[10]

Hesse G., 1973, CHROMATOGRAPHIA, V6, P277

← 1 2 →