HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF CARDENOLIDES IN DIGITALIS LEAVES AFTER SOLID-PHASE EXTRACTION

被引:47
作者
WIEGREBE, H [1 ]
WICHTL, M [1 ]
机构
[1] UNIV MARBURG,INST PHARMAZEUT BIOL,DEUTSCHHAUSSTR 17-1-2,W-3550 MARBURG,GERMANY
来源
JOURNAL OF CHROMATOGRAPHY | 1993年 / 630卷 / 1-2期
关键词
D O I
10.1016/0021-9673(93)80478-Q
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
For HPLC analysis of cardenolide glycosides of Digitalis lanata the separation of the main compounds from other constituents is useful. An improved method for doing this, based on solid-phase extraction on a C18 modified poly(styrene-divinylbenzene) polymer, is described. The presented assay permits quantitative estimation of more than 50 cardenolides in about 2 mg of dried leaf powder of Digitalis lanata with high speed and accuracy,
引用
收藏
页码:402 / 407
页数:6
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