SUB-AMBIENT AND MEDIUM-TEMPERATURE CALIBRATION

被引：8

作者：

CHARSLEY, EL

DAVIES, JP

GLOGGLER, E

HAWKINS, N

HOHNE, GWH

LEVER, T

PETERS, K

RICHARDSON, MJ

ROTHEMUND, I

STEGMAYER, A

机构：

[1] NETZSCH MASTERMIX LTD,WALSALL WS9 8UG,ENGLAND

[2] MARLIN SCI LTD,COVENTRY CV1 4LP,ENGLAND

[3] NETZSCH GERATEBAU GMBH,W-8672 SELB,GERMANY

[4] NATL PHYS LAB,TEDDINGTON TW11 0LW,MIDDX,ENGLAND

[5] UNIV ULM,KALORIMETRIE SEKT,W-7900 ULM,GERMANY

来源：

JOURNAL OF THERMAL ANALYSIS | 1993年 / 40卷 / 03期

关键词：

DSC; MELTING TRANSITIONS; REPRODUCIBLE BEHAVIOR; SOLID SOLID TRANSITIONS; TEMPERATURE CALIBRATION;

D O I：

10.1007/BF02546904

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

With some attention to temperature calibration but no other special precautions the temperatures of both solid-solid and melting transitions can be determined to within a few tenths of a Kelvin of absolute values in a range of heat-flux and power-compensation DSC instruments. Materials showing several solid-solid transitions are potentially useful multiple calibrants but require some work to define appropriate thermal treatments that lead to reproducible behaviour.

引用

页码：1405 / 1414

页数：10

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