SYNTHESIS AND CONFIGURATIONAL ASSIGNMENT OF SOME NOVEL BICYCLIC SULPHAMIDITES AND SULPHAMIDATES

被引：21

作者：

LOWE, G

REED, MA

机构：

[1] The Dyson Perrins Laboratory, Oxford University, Oxford, OX1 3QY, South Parks Road

来源：

TETRAHEDRON-ASYMMETRY | 1990年 / 1卷 / 12期

关键词：

D O I：

10.1016/S0957-4166(00)82280-6

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

(S)-Prolinol and 2(RS)-piperidine-methanol each react with thionyl chloride to give a pair of diastereoisomeric bicyclic sulphamidites which differ only in their configuration at sulphur. By contrast 2(RS)-pyrrolidine-ethanol and 2(RS)-piperidine-ethanol each react with thionyl chloride to give single diastereoisomeric products. The configurations of these bicyclic sulphamidites, and the sulphamidates derived from them, have been determined.

引用

页码：885 / 894

页数：10

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