SERENDIPITOUS DESYMMETRISATION DURING PORPHYRAZINE SYNTHESIS - AN X-RAY CRYSTALLOGRAPHIC STUDY OF 2,3,7,8,12,13,17,18-OCTAKIS(DIMETHYLAMINO)-2-SECOPORPHYRAZINE-2,3-DIONE

被引：31

作者：

MANI, NS

BEALL, LS

WHITE, AJP

WILLIAMS, DJ

BARRETT, AGM

HOFFMAN, BM

机构：

[1] NORTHWESTERN UNIV,DEPT CHEM,EVANSTON,IL 60208

[2] COLORADO STATE UNIV,DEPT CHEM,FT COLLINS,CO 80523

[3] UNIV LONDON IMPERIAL COLL SCI TECHNOL & MED,DEPT CHEM,LONDON SW7 2AY,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1994年 / 17期

关键词：

D O I：

10.1039/c39940001943

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Linstead macrocyclisation of 2,3-bis(dimethylamino)2(Z)-butenedinitrile gives [2,3,7,8,12,13,17,18-octakis(dimethylamino)porphyrazato]magnesium(II) and the title seco-porphyrazine, the structure of which is established by an X-ray crystallographic study.

引用

页码：1943 / 1944

页数：2

共 7 条

[1]

BEGLAND RW, 1974, J ORG CHEM, V29, P2341

[2] CONJUGATED MACROCYCLES .22. TETRAZAPORPHIN AND ITS METALLIC DERIVATIVES [J].