FAST HETERONUCLEAR 3-D NMR-SPECTROSCOPY

被引：14

作者：

SCHMIEDER, P

KESSLER, H

OSCHKINAT, H

机构：

[1] TECH UNIV MUNICH,INST ORGAN CHEM,LICHTENBERGSTR 4,W-8046 GARCHING,GERMANY

[2] MAX PLANCK INST BIOCHEM,W-8033 MARTINSRIED,GERMANY

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH | 1990年 / 29卷 / 05期

关键词：

D O I：

10.1002/anie.199005461

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Carbon atom correlations become interesting in 3D NMR spectroscopy if one selects CH2 groups with an inverse DEPT sequence in such a way that the spectral breadth in two of the dimensions is limited. 3 D DEPT‐TOCSY has made it possible to obtain, within about ten hours and with a very good signal‐to‐noise ratio, a high‐resolution 13C‐resolved 3D NMR spectrum of a cyclic hexapeptide. Copyright © 1990 by VCH Verlagsgesellschaft mbH, Germany

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页码：546 / 548

页数：3

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