HIGH-PERFORMANCE ION CHROMATOGRAPHY DETERMINATION OF TOTAL SULFITES IN FOODSTUFFS

被引:18
作者
RUIZ, E
SANTILLANA, MI
DEALBA, M
NIETO, MT
GARCIACASTELLANO, S
机构
[1] Servicio de Bromatología, Centro Nacional de Alimentacón, C. Majadahonda-Pozutlo, 28220 Madrid, Km.2
来源
JOURNAL OF LIQUID CHROMATOGRAPHY | 1994年 / 17卷 / 02期
关键词
D O I
10.1080/10826079408013363
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
An alternative chromatographic method based upon a combination of a modified Monnier-Williams procedure and an Ion Chromatography separation and quantitation of sulfite, have been developed. The collected gaseous SO2 is oxidized to sulfate with hydrogen peroxide. IC determination was carried out with an anion-exchange polymetacrylate column, borate/gluconate as eluent and conductivity detection. The combined method shows a good detection limit as well as a high chromatographic resolution. It is also applicable to the analysis of several foodstuffs.
引用
收藏
页码:447 / 456
页数:10
相关论文
共 14 条
[1]  
ANDERSON C, 1986, J ASSOC OFF ANA CHEM, V69, P14
[2]   ION CHROMATOGRAPHY FOR DETERMINING RESIDUAL SULFITE ON SHRIMP [J].
COOPER, PL ;
MARSHALL, MR ;
GREGORY, JF ;
OTWELL, WS .
JOURNAL OF FOOD SCIENCE, 1986, 51 (04) :924-928
[3]   SULFITE HYPERSENSITIVITY - A CRITICAL-REVIEW [J].
GUNNISON, AF ;
JACOBSEN, DW .
CRC CRITICAL REVIEWS IN TOXICOLOGY, 1987, 17 (03) :185-214
[4]  
HILLERY BR, 1989, J ASSOC OFF ANA CHEM, V72, P470
[5]  
JAMIESON DM, 1985, ANN ALLERGY, V54, P115
[6]   ANALYSIS OF FREE AND TOTAL SULFITES IN FOOD BY ION CHROMATOGRAPHY WITH ELECTROCHEMICAL DETECTION [J].
KIM, HJ ;
KIM, YK .
JOURNAL OF FOOD SCIENCE, 1986, 51 (05) :1360-1361
[7]  
KIM HJ, 1989, J ASSOC OFF ANA CHEM, V72, P266
[8]  
LAWRENCE JF, 1988, J ASSOC OFF ANA CHEM, V71, P930
[9]  
PERFETTI GA, 1989, J ASSOC OFF ANA CHEM, V72, P903
[10]   EVALUATION OF AN HPLC METHOD FOR THE DETERMINATION OF SULFITING AGENTS IN FOODS [J].
PIZZOFERRATO, L ;
QUATTRUCCI, E ;
DILULLO, G .
FOOD ADDITIVES AND CONTAMINANTS, 1990, 7 (02) :189-195