CAPILLARY ZONE ELECTROPHORESIS OF REDUCING MONOSACCHARIDES AND OLIGOSACCHARIDES AS THE BORATE COMPLEXES OF THEIR 3-METHYL-1-PHENYL-2-PYRAZOLIN-5-ONE DERIVATIVES

被引：75

作者：

HONDA, S

SUZUKI, S

NOSE, A

YAMAMOTO, K

KAKEHI, K

机构：

[1] Faculty of Pharmaceutical Sciences, Kinki University, 577, 3-4-1 Kowakae, Higashi-osaka

来源：

CARBOHYDRATE RESEARCH | 1991年 / 215卷 / 01期

关键词：

D O I：

10.1016/0008-6215(91)84018-A

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Various aldoses were derivatized to their 3-methyl-1-phenyl-2-pyrazolin-5-one derivatives and analyzed by capillary zone electrophoresis as their borate complexes. All derivatives of aldopentoses and aldohexoses were completely separated from each other in 100mM borate buffer (pH 9.5) and detected by u.v. absorption in the on-column mode. This system also provided good separation of derivatives of homologous oligoglucans having various types of interglycosidic linkages.

引用

页码：193 / 198

页数：6

共 5 条

[1] A POLYMER-HOMOLOGOUS SERIES OF SUGAR ACETATES FROM THE ACETOLYSIS OF CELLULOSE
DICKEY, EE
WOLFROM, ML
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1949, 71 (03) : 825 - 828
[2] EFFECT OF ADDITION OF ORGANIC-SOLVENT ON THE SEPARATION OF POSITIONAL ISOMERS IN HIGH-VOLTAGE CAPILLARY ZONE ELECTROPHORESIS
FUJIWARA, S
HONDA, S
[J]. ANALYTICAL CHEMISTRY, 1987, 59 (03) : 487 - 490
[3] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY OF REDUCING CARBOHYDRATES AS STRONGLY ULTRAVIOLET-ABSORBING AND ELECTROCHEMICALLY SENSITIVE 1-PHENYL-3-METHYL-5-PYRAZOLONE DERIVATIVES
HONDA, S
AKAO, E
SUZUKI, S
OKUDA, M
KAKEHI, K
NAKAMURA, J
[J]. ANALYTICAL BIOCHEMISTRY, 1989, 180 (02) : 351 - 357
[4] SIMULTANEOUS DETERMINATION OF REDUCING MONOSACCHARIDES BY CAPILLARY ZONE ELECTROPHORESIS AS THE BORATE COMPLEXES OF N-2 PYRIDYLGLYCAMINES
HONDA, S
IWASE, S
MAKINO, A
FUJIWARA, S
[J]. ANALYTICAL BIOCHEMISTRY, 1989, 176 (01) : 72 - 77
[5] YAMASHITA K, 1982, METHOD ENZYMOL, V83, P105

← 1 →