BIOACCUMULATION AND TOXIC EFFECTS OF ELEVATED LEVELS OF 3,3',4,4'-TETRACHLOROAZOBENZENE (33'44'-TCAB) TOWARDS AQUATIC ORGANISMS .1. A SIMPLE METHOD FOR THE RAPID EXTRACTION, DETECTION AND DETERMINATION OF 33'44'-TCAB IN MULTIPLE BIOLOGICAL SAMPLES

被引：2

作者：

ALLINSON, G

MORITA, M

机构：

[1] National Institute for Environmental Studies, Tsukuba City, Ibaraki, 305

来源：

CHEMOSPHERE | 1995年 / 30卷 / 02期

关键词：

3,3',4,4'-TETRACHLOROAZOBENZENE; BIOLOGICAL SAMPLE ANALYSIS; GC-HRMS;

D O I：

10.1016/0045-6535(94)00384-7

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

The polychlorinated aromatic compound 3,3',4,4'-tetrachloroazobenzene (33'44'-TCAB) is a contaminant of 3,4-dichloroaniline based herbicides, but there have been no reports of methods for the quantitative determination of 33'44'-TCAB in biological organisms, In this communication we address this knowledge gap by presenting a method for the rapid extraction, detection and determination of 33'44'-TCAB in multiple biological samples based on the alkaline decomposition of the sample followed by alumina cartridge column chromatography and GC-HRMS analysis.

引用

页码：215 / 221

页数：7

共 17 条

[1] EFFECT OF DIETARY 1,3,6,8-TETRACHLORODIBENZO-P-DIOXIN ON THE JAPANESE FRESH-WATER FISH ORYZIAS-LATIPES (MEDAKA) AND AQUATIC SNAIL INDOPLANORBIS-EXUSTUS (INDOHIRAMAKIGAI) [J].