STRUCTURE OF N,N-BIS(2,3,4,5,6-PENTAFLUOROPHENYL)OXAMIDE

被引：15

作者：

YAMAGUCHI, K ^{[1
]}

MATSUMURA, G ^{[1
]}

HAGA, N ^{[1
]}

SHUDO, K ^{[1
]}

机构：

[1] UNIV TOKYO,FAC PHARMACEUT SCI,BUNKYO KU,TOKYO 113,JAPAN

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1992年 / 48卷

关键词：

D O I：

10.1107/S0108270191009757

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

C14H2F10N2O2, M(r) = 420.16, monoclinic, P2(1)/n, a = 14.206 (1), b = 4.990 (1), c = 10.964 (3) angstrom, beta = 111.68 (1)-degrees, V = 722.3 (1) angstrom 3, Z = 2, D(x) = 1.932 Mg m-3, lambda(Cu K-alpha(1)) = 1.54050 angstrom, mu = 1.974 mm-1, F(000) = 412, T = 295 K, final R = 0.040 for 971 reflections. The midpoint of the oxamide carbon chain lies on a crystallographic inversion center. An intermolecular hydrogen bond, N-H...O [N(1)-O(3) 2.877 (2) angstrom], was observed.

引用

页码：558 / 559

页数：2