LOCAL-STRUCTURE AND SIZE EFFECTS IN NANOPHASE PALLADIUM - AN X-RAY-ABSORPTION STUDY

被引:28
作者
DEPANFILIS, S
DACAPITO, F
HAAS, V
KONRAD, H
WEISSMULLER, J
BOSCHERINI, F
机构
[1] IST NAZL FIS NUCL, LAB NAZL FRASCATI, I-00044 FRASCATI, ITALY
[2] EUROPEAN SYNCHROTRON RADIAT FACIL, GILDA CRG, CNR, F-38043 GRENOBLE, FRANCE
[3] UNIV SAARLAND, D-66121 SAARBRUCKEN, GERMANY
关键词
NANOPHASE MATERIALS; X-RAY ABSORPTION SPECTROSCOPY; X-RAY DIFFRACTION; GRAIN SIZE; GRAIN BOUNDARIES; LOCAL STRUCTURE; SIZE EFFECTS;
D O I
10.1016/0375-9601(95)00708-B
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
The connection between local structure and the grain size distribution in nanophase palladium is studied by X-ray absorption spectroscopy (XAFS) and X-ray diffraction. XAFS shows that there is a reduced average coordination number in all samples; this reduction is compatible with a size effect, contradicting previous XAFS measurements.
引用
收藏
页码:397 / 403
页数:7
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