MICROWAVE IRRADIATION IN DRY MEDIA - A NEW AND EASY METHOD FOR SYNTHESIS OF TETRAPYRROLIC COMPOUNDS

被引：59

作者：

PETIT, A

LOUPY, A

MAILLARD, P

MOMENTEAU, M

机构：

[1] CTR UNIV ORSAY,INST CHIM MOLECUL ORSAY,REACT SELECT SUPPORTS LAB,CNRS,URA 478,F-91405 ORSAY,FRANCE

[2] CTR UNIV ORSAY,INST CURIE,BIOL SECT,CNRS,URA 1387,F-91405 ORSAY,FRANCE

来源：

SYNTHETIC COMMUNICATIONS | 1992年 / 22卷 / 08期

关键词：

D O I：

10.1080/00397919208021097

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

We report a simple and quick synthesis of tetrapyrrolic macrocycle in dry media conditions, under microwave irradiation. Heating in microwave oven pyrrole and benzaldehyde adsorbed on a solid acidic support affords tetraphenylporphyrin within ten minutes with very simplified treatment and purification.

引用

页码：1137 / 1142

页数：6

共 18 条

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