FIRST SYNTHESIS OF A MACROCYCLE FROM 3,6-DIFORMYLPYRIDAZINE - X-RAY CRYSTAL-STRUCTURE OF [PB-2(4+4)](CLO4)(4)

被引：35

作者：

BROOKER, S ^{[1
]}

KELLY, RJ ^{[1
]}

SHELDRICK, GM ^{[1
]}

机构：

[1] UNIV GOTTINGEN,INST ANORGAN CHEM,D-37077 GOTTINGEN,GERMANY

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1994年 / 04期

关键词：

D O I：

10.1039/c39940000487

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Condensation of 3,6-diformylpyridazine with 1,3-diaminopropane in the presence of read(II)template ions gives the first example of a macrocycle containing pyridazine-diimine head units, and only the second example of a [4 + 4] Schiff base macrocycle; the structure of [Pb-2(4 + 4)](ClO4)4, 1, is described.

引用

页码：487 / 488

页数：2

共 16 条

[1] DICOPPER(II) COMPLEXES OF NOVEL POLYFUNCTIONAL PYRIDAZINES - CRYSTAL-STRUCTURE AND MAGNETIC-PROPERTIES OF BIS[MU-PYRIDAZINE-3,6-DICARBALDEHYDE DIOXIMATO(1-)-KAPPA-N1,N'-N2,N'']-BIS[AQUA(PERCHLORATO-KAPPA-O)COPPER(II)] [J].

ABRAHAM, F ;

LAGRENEE, M ;

SUEUR, S ;

MERNARI, B ;

BREMARD, C .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1991, (06) :1443-1447

[2] MAGNETIC-PROPERTIES OF POLYNUCLEAR COMPLEXES .2. SUPEREXCHANGE IN SOME BINUCLEAR COBALT(II) COMPLEXES [J].

BALL, PW ;

BLAKE, AB .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1974, (08) :852-859

[3] SYNTHESIS OF NEW UNSYMMETRICAL TRINUCLEATING MACROCYCLE INCORPORATING BOTH PHENOLIC AND PYRIDINE HEAD UNITS - X-RAY CRYSTAL-STRUCTURE OF ([PB2(L1)(CL)](CLO4)2)X [J].

BROOKER, S ;

CROUCHER, PD .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1993, (16) :1278-1280

[4] FORMATION OF A (4+4) SCHIFF-BASE MACROCYCLIC LIGAND BY A TEMPLATE REARRANGEMENT - CRYSTAL AND MOLECULAR-STRUCTURES OF 2 TETRANUCLEAR MANGANESE(II) COMPLEXES [J].

BROOKER, S ;

MCKEE, V ;

SHEPARD, WB ;

PANNELL, LK .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1987, (11) :2555-2562

[5]

BROOKER S, UNPUB

[6]

CHEN L, 1992, CAN J CHEM, P2709

[7] DINUCLEAR AND TETRANUCLEAR COPPER(II) COMPLEXES OF THE TETRADENTATE LIGAND 1,4-BIS(2-PYRIDYLTHIO)PHTHALAZINE - STRUCTURAL, MAGNETIC, AND ELECTROCHEMICAL STUDIES [J].

CHEN, LQ ;

THOMPSON, LK ;

BRIDSON, JN .

INORGANIC CHEMISTRY, 1993, 32 (13) :2938-2943

[8] POLYNUCLEAR COMPLEXES OF COPPER(II) WITH THE TETRA-AZA LIGAND 3,6-BIS-(2'-PYRIDYL)PYRIDAZINE (L) - CRYSTAL-STRUCTURE OF THE BROMINE DERIVATIVE [CU2L(OH)BR3]N [J].

DAPPORTO, P ;

DEMUNNO, G ;

SEGA, A ;

MEALLI, C .

INORGANICA CHIMICA ACTA-ARTICLES AND LETTERS, 1984, 83 (03) :171-176

[9] SYNTHESIS AND APPLICATION OF MACROCYCLIC AND MACROACYCLIC SCHIFF-BASES [J].

GUERRIERO, P ;

VIGATO, PA ;

FENTON, DE ;

HELLIER, PC .

ACTA CHEMICA SCANDINAVICA, 1992, 46 (11) :1025-1046

[10] X-RAY STRUCTURAL-ANALYSIS OF A TETRA-MANGANESE(II) COMPLEX OF A NEW (4X4) SCHIFF-BASE MACROCYCLE INCORPORATING A CUBANE-LIKE MN4(ALKOXY)4 CORE [J].

MCKEE, V ;

SHEPARD, WB .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1985, (03) :158-159

← 1 2 →