THE DETERMINATION OF NITRATE IN CURED MEAT-PRODUCTS - A COMPARISON OF THE HPLC UV/VIS AND CD/SPECTROPHOTOMETRIC METHODS

被引:50
作者
ALONSO, A
ETXANIZ, B
MARTINEZ, MD
机构
[1] Guipúzcoa Public Health Laboratory, San Sebastian, E-20013, Avda Navarra
来源
FOOD ADDITIVES AND CONTAMINANTS | 1992年 / 9卷 / 02期
关键词
NITRATE; SPICED SPANISH SAUSAGE; HPLC; CADMIUM; COMPARISON;
D O I
10.1080/02652039209374054
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A comparison of the traditional spectrophotometric method, with prior application of a reducing Cd column, and a high performance liquid chromatography method with an anion exchanging column for the determination of nitrate in spiced Spanish sausage, was carried out. Both methods demonstrated a high correlation. The chromatographic method proved more precise, reproducible and appropriate for routine work.
引用
收藏
页码:111 / 117
页数:7
相关论文
共 18 条
[1]  
Determination de la teneur en nitrates (Méthode de reference), Viands Et Produits à Base De Viandes, (1974)
[2]  
Davis C.E., Leffler R., Erson J.B., Soderbeg D.L., Meredith F.I., Effect of pH on absorbance of azo dye formed by reaction between nitrite and sulfanilamide/N-(Lnaphthyl) ethylenediamine in residual nitrite methods for foods, Journal of the Association of Official Analytical Chemists, 68, pp. 485-488, (1985)
[3]  
Dennis M.J., Key P.E., Papworth T., Pointer M., Massey R.C., The determination of nitrate and nitrite in cured meat by HPLC/UV, Food Additives and Contaminants, 7, pp. 455-461, (1990)
[4]  
Eggers N.J., Cattle D.L., High performance liquid chromatographic method for the determination of nitrate and nitrite in cured meat, Journal of Chromatography, 354, pp. 490-494, (1986)
[5]  
Follet M.J., Ratcliff P.W., Determination of nitrite and nitrate in meat products, Journal of the Science of Food and Agriculture, 14, pp. 138-144, (1963)
[6]  
Fudge R., Truman R.W., The nitrite contents of meat products. A survey by public analysts' laboratories in South Wales and the South West of England, Journal of the Association of Public Analysts, 11, pp. 19-27, (1973)
[7]  
Hunt J., Seymour D.J., Methods for measuring nitrate-nitrogen in vegetables using anion-exchange high performance liquid chromatography, Analyst, 110, pp. 131-133, (1985)
[8]  
Scientific Status Summary: Nitrate, nitrite and nitroso compounds in foods, Food Technology, 41, pp. 127-136, (1987)
[9]  
Iskandarani Z., Pietrzyk D.J., Determination of nitrite and nitrate in water and food samples by ion interaction chromatography, Journal of the American Chemical Society, 54, pp. 2601-2603, (1982)
[10]  
Jackson P.E., Haddad P.R., Dilli S., Determination of nitrate and nitrite in cured meats using high-performance liquid chromatography, Journal of Chromatography, 295, pp. 471-478, (1984)