DETERMINATION OF DELTAMETHRIN LEVELS IN WOOL BY REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：5

作者：

DARWISH, A

机构：

[1] CSIRO Division of Animal Health, McMaster Laboratory, Glebe, New South Wales, 2037

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY | 1994年 / 17卷 / 19期

关键词：

D O I：

10.1080/10826079408013612

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A method is described for the extraction and analysis of deltamethrin in wool after pour-on or plunge dipping application. Acetonitrile was used for extraction followed by simple clean-up on Florisil or C18 cartridges. Deltamethrin levels were determined by liquid scintillation spectrometry of [C-14]-deltamethrin and high performance liquid chromatography at 217-222 nm Results showed good recovery and correlation between the two methods. This extraction procedure is relatively simple and rapid, it eliminates the need for prolonged liquid-liquid extraction and solid-phase steps thus making it more suitable for pharmacokinetic studies.

引用

页码：4215 / 4228

页数：14

共 10 条

[1]

BAYVEL ACD, 1981, WOOL TECH SHEEP BREE, V29, P17

[2] RESIDUES OF CYPERMETHRIN IN MILK FROM COWS WEARING IMPREGNATED EAR TAGS [J].