ISOLATION OF FULLERENE PRODUCTS FROM FLAMES - STRUCTURE AND SYNTHESIS OF THE C60-CYCLOPENTADIENE ADDUCT

被引：121

作者：

ROTELLO, VM

HOWARD, JB

YADAV, T

CONN, MM

VIANI, E

GIOVANE, LM

LAFLEUR, AL

机构：

[1] MIT,DEPT CHEM ENGN,CAMBRIDGE,MA 02139

[2] MIT,CTR ENVIRONM HLTH SCI,CAMBRIDGE,MA 02139

来源：

TETRAHEDRON LETTERS | 1993年 / 34卷 / 10期

关键词：

D O I：

10.1016/0040-4039(93)85006-I

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A C60-C5H6 adduct was isolated from a low pressure benzene flame. The structure of this product is identical to the Diels-Alder adduct of C60 and cyclopentadiene as established through independent synthesis. This product was determined to be adduct 1 through C-13 and proton NMR, as well as infrared and mass spectrometry.

引用

页码：1561 / 1562

页数：2

共 7 条

[1] ANACLETO JF, IN PRESS RAPID COMMU
[2] 2D NUCLEAR-MAGNETIC-RESONANCE ANALYSIS OF OSMYLATED C60
HAWKINS, JM
LOREN, S
MEYER, A
NUNLIST, R
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1991, 113 (20) : 7770 - 7771
[3] PRODUCTION OF C-60 AND C-70 FULLERENES IN BENZENE OXYGEN FLAMES
HOWARD, JB
MCKINNON, JT
JOHNSON, ME
MAKAROVSKY, Y
LAFLEUR, AL
[J]. JOURNAL OF PHYSICAL CHEMISTRY, 1992, 96 (16) : 6657 - 6662
[4] FULLERENES C60 AND C70 IN FLAMES
HOWARD, JB
MCKINNON, JT
MAKAROVSKY, Y
LAFLEUR, AL
JOHNSON, ME
[J]. NATURE, 1991, 352 (6331) : 139 - 141
[5] PEREAULT H, 1992, RAPID COMMUN MASS SP, V6, P214
[6] DIHYDROFULLEROID H2C61 - SYNTHESIS AND PROPERTIES OF THE PARENT FULLEROID
SUZUKI, T
LI, QC
KHEMANI, KC
WUDL, F
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (18) : 7301 - 7302
[7] WUDL F, 1992, ACS SYM SER, V481, P161

← 1 →