SEPARATION OF SULFUR-CONTAINING CHEMICAL WARFARE RELATED-COMPOUNDS IN AQUEOUS SAMPLES BY MICELLAR ELECTROKINETIC CHROMATOGRAPHY

被引：29

作者：

CHEICANTE, RL

STUFF, JR

DURST, HD

机构：

[1] EAI CORP,ABINGDON,MD 21009

[2] USA,MAT COMMAND TREATY LAB,EDGEWOOD,MD 21005

来源：

JOURNAL OF CHROMATOGRAPHY A | 1995年 / 711卷 / 02期

关键词：

D O I：

10.1016/0021-9673(95)00524-Q

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A method is described in which micellar electrokinetic chromatography (MEKC) is used to separate thiodiglycol, 2,2'-sulfinyldiethanol, 1,4-dithiane, 1,4-thioxane, O-isobutyl methylphosphonothioic acid and O-ethyl methylphosphonothioic acid in aqueous samples. Detection limits range from 1 to 10 mu g/ml and the calibration curves are linear over two orders of magnitude. The compounds are separated in under 10 min. The method fulfills our requirements for a rapid, on-site screening technique for these compounds.

引用

页码：347 / 352

页数：6

共 13 条

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